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Calibration

CaRo 11   (Calibration-Round-Robin  2011)

for determination of the explosion characteristics of dusts

 

K_PDF.gif     CaRo11 Progress     (19. January 2012)


Goal:  Determination of the explosion characteristics using standard test methods:
·          Pmax maximum explosion overpressure
·          Kmax product-specific constant
·          MIE minimum ignition energy
           and calibration of the relevant test apparatus.

Reason: According to international standards (e.g. ISO 9000, GLP), test equipment must be calibrated at intervals by comparison with a standard or a calibrated testing apparatus.
This calibration also applies to the 20-l-apparatus and the 1-m3-vessel for the determination of Pmax and Kmax and the apparatus for determination of the minimum ignition energy. The test procedure is an important part of this calibration. A general check at the component level is incomplete and hence inadmissible.
Unfortunately there are neither internationally recognized reference samples nor reference equipment available for the determination of these explosion characteristics. Therefore, a calibration round robin test (CaRo) will be carried out every two years.

Calibration method
: The mean values of the explosion indices, measured by the par­ticipating laboratories, will be calculated as reference values. All apparatus, with results lying within the given tolerance range, meet the calibration requirements and will receive a calibration-certificate from us.
Based on experience with previous round robin tests, we are certain that we will be able to discover and rectify the cause of any errors with installations producing results differing widely from the reference values.

 

Our service: The test dust will be selected, homogenized, packed under nitrogen and mailed by us. Additionally we supply with the test dust preliminary reference-results (20-l-apparatus and MIKE 3 minimum ignition energy apparatus). Therefore you will be able to pre-check your own test results. On elapse of the test deadline, a detailed overall evalua­tion with calculation of the standard values and the associated tolerance range will be made. Those laboratories which meet the calibration requirements will receive a certificate. All results will then be summarized in tabular form (anonymously) and mailed to the participants.
 

Costs: The flat charges depend on the number of apparatuses to be tested::

Order No.  Testing of price in CHF  price in EUR
SP 8925 1  apparatus 2000.-  1600.-
SP 8926 2  apparatuses 3050.-  2440.-
SP 8927 3  apparatuses 3780.- 3024.-

The price includes packaging, but not the VAT (value added tax).

Test dust:   The amount of test dust depends on the type of apparatus.
20-l-apparatus,  MIE-apparatus:      1kg
1m3-vessel:     10kg   (SP8928 extra costs = CHF 1420.- / EUR 1136.-)

Schedule: 

Deadline for receipt of test results:  end of Year 2011
Final report of CaRo 11, certificates: January 2012
Next Calibration-Round-Robin CaRo 13: 2013

 

 
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